Temperature range: RT to 450°C (can be shifted using add. equipment)
Heating rates: 0-180K/min (AC-Mode), 35-20'000K/s (Burst Mode, < 10 s duration)
Buffer: 2 mega-samples; Sampling rate: up to 40khz

Sample: solid; sample mass < 0.5µg
max sample size < 60 x 60 x 15 µm³ 

Xray-technique: suitable for transmission geometries; partially compatible with reflection geometry

Special introduction to the functioning of the device is required, MEMS need to be calibrated before use (to be done in collaboration with the beamline personel)

(1) Square hole pattern (M3) 40 x 40 mm raster (height to beam 30mm)
(2) Square hole pattern (M2) 14 x 14 mm raster (height to beam 82mm)

ID13NanoCalorimeter1.jpg

MEMS nano-heater / Nano calorimeter

ID13NanoCalorimeter2.jpg

Nano calorimeter on the BL

ID13NanoCalorimeter3.jpg

Nano calorimeter on the BL

 

ID13 - MICROFOCUS BEAMLINE