Capillary oven (1)
Capillary oven
Temperature max = 1000°C
control: power supply Delta Electronica (model SM 7020 D) + Eurotherm controller 2408 + thermocouple type K
Tmax = 1000 C ; ramping: 5 - 10 C / min
oven design: resistive Kanthal heater, sandwich geometry
Sample size: flat, 20 x 20 mm2, thick = 5; round, diam = 6 mm, L~ 20 mm
sample slot width = 50 x 12mm; exit opening = 20 mm; 2theta= 20 degr.
Capilary oven
https://journals.iucr.org/j/issues/2014/01/00/rg5045/rg5045.pdf