Appendix
Column list from TEMPERATURE SCANS as of Jan. 30,2003
Scattering angle – Q relation and angular spacing of analysers
High Resolution Si(h h h ) monochromator and useful conversions
Column list from TEMPERATURE SCANS as of Jan. 30,2003
Col# | Counter name | Counter meaning | Inv.# |
---|---|---|---|
1 | Temperature | monot setpoint | -40 |
2 | H | -39 | |
3 | K | -38 | |
4 | L | -37 | |
5 | Epoch | -36 | |
6 | sec | integration time | -35 |
7 | pindiode | -34 | |
8 | izero OH2 | pmoni | -33 |
9 | izero EH1 | izero (mon. after ML) | -32 |
10 | Ione/Izero | -31 | |
11 | Sec | -30 | |
12 | Prema_ad5 | NTC mono in | -29 |
13 | Prema_ad6 | NTC analyzer #1 | -28 |
14 | Prema_ad7 | NTC analyzer #2 | -27 |
15 | Prema_ad8 | NTC analyzer #3 | -26 |
16 | Prema_ad9 | NTC analyzer #4 | -25 |
17 | Prema_ad10 | NTC analyzer #5 | -24 |
18 | Prema_ad11 | NTC analyzer #6 | -23 |
19 | Prema_ad12 | NTC analyzer #7 | -22 |
20 | Prema_ad13 | NTC analyzer #8 | -21 |
21 | Prema_ad14 | NTC analyzer #9 | -20 |
22 | Prema_ad16 | NTC EH1 | -19 |
23 | pico | -18 | |
24 | deta1 | -17 | |
25 | deta2 | -16 | |
26 | deta3 | -15 | |
27 | deta4 | -14 | |
28 | deta5 | -13 | |
29 | SR current | -12 | |
30 | NTC_mono | mono temp. in C | -11 |
31 | Cryostat | T2 (sample) in displex | -10 |
32 | newdet | S(Q)-det near Ana2 | -9 |
33 | prema_ad15 | PT100 chamber 7m | -8 |
34 | ione | monitor after slits | -7 |
35 | detsq | S(Q) near sample | -6 |
36 | deta6 | -5 | |
37 | deta7 | -4 | |
38 | deta8 | -3 | |
39 | deta9 | -2 | |
40 | Imirr | monitor before ML | -1 |
Scattering angle – Q relation and angular spacing of analysers
Si(8 8 8)
Q [nm-1] = 4/ * sin(2/2) = 160.3 nm-1 *sin(2/2)
2 (10 nm-1) = 7.153° = 0.7839 Å E = 15.816 keV
Analyzer No° | tth [°] |
---|---|
1 | 8.730° |
2 | 7.153° |
3 | 5.645° |
4 | 4.095° |
5 | 2.527° |
Si(9 9 9)
Q = 180.35 * sin(2/2)
2 (10 nm-1) = 6.357° = 0.6968 Å E = 17.794 keV
Analyzer No° | tth [°] |
---|---|
1 | 7.934° |
2 | 6.357° |
3 | 4.849° |
4 | 3.299° |
5 | 1.731° |
Si(11 11 11)
Q = 220.414 * sin(2/2)
2 (10 nm-1) = 5.200° = 0.5701 Å E = 21.7477 keV
Analyzer No° | tth [°] |
---|---|
1 | 6.777° |
2 | 5.200° |
3 | 3.692° |
4 | 2.142° |
5 | 0.574° |
Relative tth between analyzers
#2 | #3 | #4 | #5 | |
---|---|---|---|---|
#1 | -1.577° | 3.085° | 4.635° | 6.203° |
#2 | 1.508° | 3.058° | 4.626° | |
#3 | 1.550° | 3.118° | ||
#4 | 1.568° |
Maximum momentum transfer and “Q-spacing”
Energy[keV] | Reflection order n | Qmax (7 m)[nm-1] | Q (7 m) [nm-1] | Qmax (12 m)[nm-1] | Q (12 m)[nm-1] |
---|---|---|---|---|---|
13.840 | 7 | 64 | 1.89 | 30.3 | 1.89 |
15.817 | 8 | 74 | 2.16 | 35 | 2.16 |
17.794 | 9 | 83 | 2.43 | 39 | 2.43 |
21.747 | 11 | 101 | 3.00 | 47 | 3.00 |
23.725 | 12 | 111 | 3.24 | 52 | 3.24 |
25.704 | 13 | 120 | 3.50 | 56 | 3.50 |
Maximum momentum transfer, Qmax, for the 7- and 12-meter section of the spectrometer arm. Q indicates the Q-spacing between adjacent analysers. If the two sections are utilised simultaneously, The Q-spacing is reduced to half of the indicated value.
High Resolution Si(h h h ) monochromator and useful conversions
Reflection | (7 7 7) | (8 8 8) | (9 9 9) | (11 11 11) | (12 12 12) | (13 13 13) |
Wavelength [Å-1] |
0.895886 | 0.7839003 | 0.6968003 | 0.5701093 | 0.52260096 | 0.48240018 |
Energy [eV] |
13839.35 | 15816.40 | 17793.45 | 21747.556 | 23724.572 | 25701.6568 |
Conversion meV -> K |
0.02822 | 0.02470 | 0.02195 | 0.01796 | 0.01646 | 0.01520 |
(E)M [meV] | 5.3 | 4.4 | 2.2 | 1.02 | 0.73 | 0.5 |
(E/E)M | 3.8*10-7 | 2.8*10-7 | 1.2*10-7 | 4.7*10-8 | 3.0*10-8 | 2.0*10-8 |
Conversion angles -> nm-1 | 140.265 | 160.306 | 180.344 | 220.424 | 240.459 | 260.497 |
QMax [Å-1] (for 7m arm) |
5.93 | 6.77 | 7.62 | 9.32 | 10.16 | 11.00 |
Flux [ph/s 200 mA] |
7*1010 | 6*1010 | 1.8*1010 | 4.4*1010 | 3.9*1010 | 9.8*1010 |