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Identification of the Calcium, Aluminum, and Magnesium Distribution within Millimeter-Sized Extraterrestrial Materials Using Nonresonant X-ray Raman Spectroscopy in Preparation for the Hayabusa2 Sample Return Mission. Tack P, De Pauw E, Tkalcec B, Longo A, Sahle CJ, Brenker F & Vincze L. Analytical Chemistry93, 14651–14658 (2021) https://doi.org/10.1021/acs.analchem.1c02774
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Insight into the effect of different thermal treatment routes on the microstructure of AlSi7Mg produced by laser powder bed fusion. Casati R, Coduri M, Checchia S & Vedani M. Materials Characterization172, 110881 (2021) https://doi.org/10.1016/j.matchar.2021.110881
Lithium distribution and transfer in high-power 18650-type Li-ion cells at multiple length scales. Petz D, Mühlbauer MJ, Baran V, Schökel A, Kochetov V, Hofmann M, Dyadkin V, Staron P, Vaughan G, Lienert U, Müller-Buschbaum P & Senyshyn A. Energy Storage Materials41, 546–553 (2021) https://doi.org/10.1016/j.ensm.2021.06.028
Mapping the coke formation within a zeolite catalyst extrudate in space and time by operando computed X-ray diffraction tomography. Wragg DS, Kalantzopoulos GN, Pappas DK, Pinilla-Herrero I, Rojo-Gama D, Redekop E, Di Michiel M, Beato P, Lundegaard LF & Svelle S. Journal of Catalysis401, 1–6 (2021) https://doi.org/10.1016/j.jcat.2021.07.001
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Morphogenesis of Magnetite Mesocrystals: Interplay between Nanoparticle Morphology and Solvation Shell. Schlotheuber né Brunner J et al.Chemistry of Materials33, 9119–9130 (2021) https://doi.org/10.1021/acs.chemmater.1c01941
Multi-length scale 5D diffraction imaging of Ni–Pd/CeO 2 –ZrO 2 /Al 2 O 3 catalyst during partial oxidation of methane. Matras D, Vamvakeros A, Jacques SDM, Michiel M di, Middelkoop V, Ismagilov IZ, Matus EV, Kuznetsov VV, Cernik RJ & Beale AM. Journal of Materials Chemistry A9, 11331–11346 (2021) https://doi.org/10.1039/D1TA01464A
Multi-Scale Studies of 3D Printed Mn–Na–W/SiO2 Catalyst for Oxidative Coupling of Methane. Karsten T, Middelkoop V, Matras D, Vamvakeros A, Poulston S, Grosjean N, Rollins B, Gallucci F, Godini HR, Jacques SDM, Beale AM & Repke J-U. Catalysts11, 290 (2021) https://doi.org/10.3390/catal11030290
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Polarimetry With a Multilayer CdTe Prototype for Soft Gamma-Ray Astrophysics. Moita M, Curado da Silva RM, Maia JM, Caroli E, Virgilli E, Auricchio N, Stephen JB, Frontera F & Sordo S del. IEEE Transactions on Nuclear Science68, 2655–2660 (2021) https://doi.org/10.1109/TNS.2021.3110472
Quantifying the hydroxyapatite orientation near the ossification front in a piglet femoral condyle using X-ray diffraction tensor tomography. Mürer FK, Chattopadhyay B, Madathiparambil AS, Tekseth KR, Di Michiel M, Liebi M, Lilledahl MB, Olstad K & Breiby DW. Scientific Reports11, 2144 (2021) https://doi.org/10.1038/s41598-020-80615-4
Real-time tomographic diffraction imaging of catalytic membrane reactors for the oxidative coupling of methane. Vamvakeros A, Matras D, Jacques SDM, Michiel M di, Middelkoop V, Cong P, Price SWT, Bull CL, Senecal P & Beale AM. Catalysis Today364, 242–255 (2021) https://doi.org/10.1016/j.cattod.2020.05.045
Reduction of PdO/Al 2 O 3 in Liquid Cyclohexane Followed In Situ by ATR-IR, High-Energy XRD, and XAS. Fovanna T, Alxneit I, Clark AH, Checchia S, Di Michiel M, Kröcher O, Nachtegaal M & Ferri D. The Journal of Physical Chemistry C125, 16473–16482 (2021) https://doi.org/10.1021/acs.jpcc.1c01882
The Application of HEXS and HERFD XANES for Accurate Structural Characterisation of Actinide Nanomaterials: The Case of ThO2. Amidani L, Vaughan GBM, Plakhova TV, Romanchuk AYu, Gerber E, Svetogorov R, Weiss S, Joly Y, Kalmykov SN & Kvashnina KO. Chemistry (Weinheim an Der Bergstrasse, Germany)27, 252–263 (2021) https://doi.org/10.1002/chem.202003360
The Effect of Specimen Size and Test Procedure on the Creep Behavior of ME21 Magnesium Alloy. Camin B & Gille M. Crystals11, 918 (2021) https://doi.org/10.3390/cryst11080918
4D imaging of lithium-batteries using correlative neutron and X-ray tomography with a virtual unrolling technique. Ziesche RF, Arlt T, Finegan DP, Heenan TM, Tengattini A, Baum D, Kardjilov N, Markötter H, Manke I & Kockelmann W. Nature communications11, 1–11 (2020)
Complex geometric structure of a simple solid-liquid interface: Gan (0001)-ga. Jong A de, Vonk V, Boćkowski M, Grzegory I, Honkimäki V & Vlieg E. Physical review letters124, 086101 (2020)
CuO/La 0.5 Sr 0.5 CoO 3: precursor of efficient NO reduction catalyst studied by operando high energy X-ray diffraction under three-way catalytic conditions. Alxneit I, Garbujo A, Carollo G, Ferri D & Glisenti A. Physical Chemistry Chemical Physics22, 18798–18805 (2020)
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Effects of Nanodomains on Local and Long-Range Phase Transitions in Perovskite-Type Eu0. 8Ca0. 2TiO3–δ. Widenmeyer M, Checchia S, Xiao X, Scavini M & Weidenkaff A. Nanomaterials10, 769 (2020)
Electric-field-induced phase transformation and frequency-dependent behavior of bismuth sodium titanate–barium titanate. Lee K-Y, Shi X, Kumar N, Hoffman M, Etter M, Checchia S, Winter J, Lemos da Silva L, Seifert D & Hinterstein M. Materials13, 1054 (2020)
Energy and Environmental Science at ESRF. Longo A, Sahle CJ, Glatzel P, Giacobbe C, Rack A, Mathon O, Lomachenko K, Segura-Ruiz J, Villanova J & Castillo-Michel H. Synchrotron Radiation News33, 40–51 (2020)
Exploring cycling induced crystallographic change in NMC with X-ray diffraction computed tomography. Daemi SR, Tan C, Vamvakeros A, Heenan TM, Finegan DP, Di Michiel M, Beale AM, Cookson J, Petrucco E & Weaving JS. Physical Chemistry Chemical Physics22, 17814–17823 (2020)
Fast operando X-ray pair distribution function using the DRIX electrochemical cell. Diaz-Lopez M, Cutts GL, Allan PK, Keeble DS, Ross A, Pralong V, Spiekermann G & Chater PA. Journal of Synchrotron Radiation27, (2020)
Functional surface layers in relaxor ferroelectrics. Kumar N, Kong S, Sharma P, Shi X, Vats G, Checchia S, Seidel J, Hoffman M & Daniels J. Journal of Materials Chemistry C8, 7663–7671 (2020)
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High Speed In Situ Synchrotron Observation of Cyclic Deformation and Phase Transformation of Superelastic Nitinol at Ultrasonic Frequency. Fitzka M, Rennhofer H, Catoor D, Reiterer M, Lichtenegger H, Checchia S, Michiel M di, Irrasch D, Gruenewald T & Mayer H. Experimental Mechanics60, 317–328 (2020)
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In situ X-ray diffraction computed tomography studies examining the thermal and chemical stabilities of working Ba 0.5 Sr 0.5 Co 0.8 Fe 0.2 O 3− δ membranes during oxidative coupling of methane. Matras D, Vamvakeros A, Jacques SD, Middelkoop V, Vaughan G, Aran MA, Cernik RJ & Beale AM. Physical Chemistry Chemical Physics22, 18964–18975 (2020)
Mechanochemical Metathesis between AgNO3 and NaX (X= Cl, Br, I) and Ag2XNO3 Double-Salt Formation. Lukin S, Stolar T, Lončarić I, Milanović I, Biliškov N, Michiel M di, Friščić T & Halasz I. Inorganic Chemistry59, 12200–12208 (2020)
Multiscale investigation of adsorption properties of novel 3D printed UTSA-16 structures. Grande CA, Blom R, Middelkoop V, Matras D, Vamvakeros A, Jacques SD, Beale AM, Di Michiel M, Andreassen KA & Bouzga AM. Chemical Engineering Journal402, 126166 (2020)
Nanoscale imaging of shale fragments with coherent X-ray diffraction. Chattopadhyay B, Madathiparambil AS, Mürer FK, Cerasi P, Chushkin Y, Zontone F, Gibaud A & Breiby DW. Journal of applied crystallography53, (2020)
Operando investigation of the lithium/sulfur battery system by coupled X-ray absorption tomography and X-ray diffraction computed tomography. Tonin G, Vaughan GB, Bouchet R, Alloin F, Di Michiel M & Barchasz C. Journal of Power Sources468, 228287 (2020)
Pd-LaFeO3 catalysts in aqueous ethanol: Pd reduction, leaching, and structural transformations in the presence of a base. Checchia S, Mulligan CJ, Emerich H, Alxneit I, Krumeich F, Di Michiel M, Thompson PB, Hii KKM, Ferri D & Newton MA. ACS Catalysis10, 3933–3944 (2020)
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Real-time multi-length scale chemical tomography of fixed bed reactors during the oxidative coupling of methane reaction. Vamvakeros A, Matras D, Jacques SD, Michiel M di, Price SW, Senecal P, Aran MA, Middelkoop V, Stenning GB & Mosselmans JFW. Journal of Catalysis386, 39–52 (2020)
Spatial dynamics of lithiation and lithium plating during high-rate operation of graphite electrodes. Finegan DP, Quinn A, Wragg DS, Colclasure AM, Lu X, Tan C, Heenan TM, Jervis R, Brett DJ & Das S. Energy & Environmental Science13, 2570–2584 (2020)
Spatial quantification of dynamic inter and intra particle crystallographic heterogeneities within lithium ion electrodes. Finegan DP, Vamvakeros A, Tan C, Heenan TM, Daemi SR, Seitzman N, Di Michiel M, Jacques S, Beale AM & Brett DJ. Nature communications11, 1–11 (2020)
Temperature evolution of the bulk nano-structure in a homologous series of room temperature ionic liquids. Pontoni D, DiMichiel M & Deutsch M. Journal of Molecular Liquids300, 112280 (2020)
The Detection of Monoclinic Zirconia and Non-Uniform 3D Crystallographic Strain in a Re-Oxidized Ni-YSZ Solid Oxide Fuel Cell Anode. Heenan TM, Vamvakeros A, Tan C, Finegan DP, Daemi SR, Jacques SD, Beale AM, Di Michiel M, Brett DJ & Shearing PR. Crystals10, 941 (2020)
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The missing pieces of the PuO 2 nanoparticle puzzle. Gerber E, Romanchuk AY, Pidchenko I, Amidani L, Rossberg A, Hennig C, Vaughan GB, Trigub A, Egorova T & Bauters S. Nanoscale12, 18039–18048 (2020)
Using In-Situ Laboratory and Synchrotron-Based X-ray Diffraction for Lithium-Ion Batteries Characterization: A Review on Recent Developments. Llewellyn AV, Matruglio A, Brett DJ, Jervis R & Shearing PR. Condensed Matter5, 75 (2020)
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Operando and Postreaction Diffraction Imaging of the La–Sr/CaO Catalyst in the Oxidative Coupling of Methane Reaction. Matras D, Jacques SDM, Poulston S, Grosjean N, Estruch Bosch C, Rollins B, Wright J, Di Michiel M, Vamvakeros A, Cernik RJ & Beale AM. The Journal of Physical Chemistry C123, 1751–1760 (2019) https://doi.org/10.1021/acs.jpcc.8b09018
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Synchrotron pair distribution function analyses of ye’elimite-based pastes. Cuesta A, Zea-Garcia JD, De la Torre AG, Santacruz I & Aranda MAG. Advances in Cement Research31, 138–146 (2019) https://doi.org/10.1680/jadcr.18.00097
Convenient Preparation of Graphene Oxide from Expandable Graphite and Its Characterization by Positron Annihilation Lifetime Spectroscopy. Panzarasa G, Consolati G, Scavini M, Longhi M & Quasso F. C — Journal of Carbon Research5, 6 (2019) https://doi.org/10.3390/c5010006
Quantifying fatigue overload retardation mechanisms by energy dispersive X-ray diffraction. C.a S, S K, P L-C, M M, T C & P.j W. Journal of the Mechanics and Physics of Solids124, 392–410 (2019) https://doi.org/10.1016/j.jmps.2018.10.020
Deformation behavior of lean duplex stainless steels with strain induced martensitic transformation: Role of deformation mechanisms, alloy chemistry and predeformation. Lechartier A, Meyer N, Estevez R, Mantel M, Martin G, Parry G, Veron M & Deschamps A. Materialia5, 100190 (2019) https://doi.org/10.1016/j.mtla.2018.100190
Control of Pharmaceutical Cocrystal Polymorphism on Various Scales by Mechanochemistry: Transfer from the Laboratory Batch to the Large-Scale Extrusion Processing. Stolar T, Lukin S, Tireli M, Sović I, Karadeniz B, Kereković I, Matijašić G, Gretić M, Katančić Z, Dejanović I, Michiel M di, Halasz I & Užarević K. ACS Sustainable Chemistry & Engineering7, 7102–7110 (2019) https://doi.org/10.1021/acssuschemeng.9b00043
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Design of next-generation ceramic fuel cells and real-time characterization with synchrotron X-ray diffraction computed tomography. Li T, Heenan TMM, Rabuni MF, Wang B, Farandos NM, Kelsall GH, Matras D, Tan C, Lu X, Jacques SDM, Brett DJL, Shearing PR, Di Michiel M, Beale AM, Vamvakeros A & Li K. Nature Communications10, 1497 (2019) https://doi.org/10.1038/s41467-019-09427-z
In-depth study of the mechanism of heavy metal trapping on the surface of hydroxyapatite. Ferri M, Campisi S, Scavini M, Evangelisti C, Carniti P & Gervasini A. Applied Surface Science475, 397–409 (2019) https://doi.org/10.1016/j.apsusc.2018.12.264
Quantifying Reaction and Rate Heterogeneity in Battery Electrodes in 3D through Operando X-ray Diffraction Computed Tomography. Liu H, Kazemiabnavi S, Grenier A, Vaughan G, Di Michiel M, Polzin BJ, Thornton K, Chapman KW & Chupas PJ. ACS Applied Materials & Interfaces11, 18386–18394 (2019) https://doi.org/10.1021/acsami.9b02173
Structural and electronic changes in graphite fluorides as a function of fluorination rate: An XRS, PDF and DFT study. Cavallari C, Brunelli M, Radescu S, Dubois M, Batisse N, Vaughan GBM, Fischer HE & Pischedda V. Carbon147, 1–8 (2019) https://doi.org/10.1016/j.carbon.2019.02.053
Spatially Resolving Lithiation in Silicon–Graphite Composite Electrodes via in Situ High-Energy X-ray Diffraction Computed Tomography. Finegan DP, Vamvakeros A, Cao L, Tan C, Heenan TMM, Daemi SR, Jacques SDM, Beale AM, Di Michiel M, Smith K, Brett DJL, Shearing PR & Ban C. Nano Letters19, 3811–3820 (2019) https://doi.org/10.1021/acs.nanolett.9b00955
On isothermality in some commonly used plug flow reactors for X-ray based investigations of catalysts. Newton MA, Checchia S, Knorpp AJ, Stoian D, Beek W van, Emerich H, Longo A & Bokhoven JA van. Catalysis Science & Technology9, 3081–3089 (2019) https://doi.org/10.1039/C9CY00464E
Interfacial Stereocomplexation To Strengthen Fused Deposition Modeled Poly(lactide) Welds. Srinivas V, Hooy-Corstjens CSJ van, Vaughan GBM, Leeuwen B van, Rastogi S & Harings JAW. ACS Applied Polymer Materials1, 2131–2139 (2019) https://doi.org/10.1021/acsapm.9b00421
Sustainable iron-based oxygen carriers for hydrogen production – Real-time operando investigation. De Vos Y, Vamvakeros A, Matras D, Jacobs M, Van Der Voort P, Van Driessche I, Jacques S, Middelkoop V & Verberckmoes A. International Journal of Greenhouse Gas Control88, 393–402 (2019) https://doi.org/10.1016/j.ijggc.2019.06.016
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Influence of high hydrostatic pressure on solid supported DPPC bilayers with hyaluronan in the presence of Ca2+ ions. Zander T, Wieland DCF, Raj A, Salmen P, Dogan S, Dėdinaitė A, Garamus VM, Schreyer A, Claesson PM & Willumeit-Römer R. Soft Matter15, 7295–7304 (2019) https://doi.org/10.1039/C9SM01066A
In situ through-thickness analysis of crack tip fields with synchrotron X-ray diffraction. Lopez-Crespo P, Peralta JV, Kelleher JF & Withers PJ. International Journal of Fatigue127, 500–508 (2019) https://doi.org/10.1016/j.ijfatigue.2019.06.029
3D printed Ni/Al2O3 based catalysts for CO2 methanation - a comparative and operando XRD-CT study. Middelkoop V, Vamvakeros A, Wit D de, Jacques SDM, Danaci S, Jacquot C, Vos Y de, Matras D, Price SWT & Beale AM. Journal of CO2 Utilization33, 478–487 (2019) https://doi.org/10.1016/j.jcou.2019.07.013
Cultural and Natural Heritage at the ESRF: Looking Back and to the Future. Cotte M, Autran P-O, Berruyer C, Dejoie C, Susini J & Tafforeau P. Synchrotron Radiation News32, 34–40 (2019) https://doi.org/10.1080/08940886.2019.1680213
Soft Templating and Disorder in an Applied 1D Cobalt Coordination Polymer Electrocatalyst. Triana CA, Moré R, Bloomfield AJ, Petrović PV, Ferrón SG, Stanley G, Zarić SD, Fox T, Brothers EN, Sheehan SW, Anastas PT & Patzke GR. Matter1, 1354–1369 (2019) https://doi.org/10.1016/j.matt.2019.06.021
On the Origin of the Anisotropic Damage of X100 Line Pipe Steel: Part I—In Situ Synchrotron Tomography Experiments. Madi Y, Garcia J-M, Proudhon H, Shinohara Y, Helfen L, Besson J & Morgeneyer TF. Integrating Materials and Manufacturing Innovation8, 570–596 (2019) https://doi.org/10.1007/s40192-019-00165-0
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Identifying the Cause of Rupture of Li-Ion Batteries during Thermal Runaway. Finegan DP, Darcy E, Keyser M, Tjaden B, Heenan TMM, Jervis R, Bailey JJ, Vo NT, Magdysyuk OV, Drakopoulos M, Michiel MD, Rack A, Hinds G, Brett DJL & Shearing PR. Advanced Science5, 1700369 (2018) https://doi.org/10.1002/advs.201700369
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X-ray physico-chemical imaging during activation of cobalt-based Fischer–Tropsch synthesis catalysts. Beale AM, Jacques SDM, Di Michiel M, Mosselmans JFW, Price SWT, Senecal P, Vamvakeros A & Paterson J. Philosophical Transactions of the Royal Society A: Mathematical, Physical and Engineering Sciences376, 20170057 (2018) https://doi.org/10.1098/rsta.2017.0057
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From light to heavy alkali metal tetraphosphonates (M = Li, Na, K, Rb, Cs): cation size-induced structural diversity and water-facilitated proton conductivity. Salcedo IR, Colodrero RMP, Bazaga-García M, Vasileiou A, Papadaki M, Olivera-Pastor P, Infantes-Molina A, Losilla ER, Mezei G, Cabeza A & Demadis KD. CrystEngComm20, 7648–7658 (2018) https://doi.org/10.1039/C8CE01351A
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Chemical Structures of Specific Sodium Ion Battery Components Determined by Operando Pair Distribution Function and X‐ray Diffraction Computed Tomography. Sottmann J, Di Michiel M, Fjellvåg H, Malavasi L, Margadonna S, Vajeeston P, Vaughan GB & Wragg DS. Angewandte Chemie International Edition56, 11385–11389 (2017)
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Observation of crack growth in a polycrystalline ferroelectric by synchrotron X-ray diffraction. Huber J, Hofmann F, Barhli S, Marrow T & Hildersley C. Scripta materialia140, 23–26 (2017)
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Phase analysis of NiTi wire based on synchrotron 2D X-ray diffraction pattern in Matlab. Dudr M, Šimek D & Drahokoupil J. Acta Polytechnica CTU Proceedings9, 8–12 (2017)
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Real-time scattering-contrast imaging of a supported cobalt-based catalyst body during activation and Fischer–Tropsch synthesis revealing spatial dependence of particle size and phase on catalytic properties. Senecal P, Jacques SD, Di Michiel M, Kimber SA, Vamvakeros A, Odarchenko Y, Lezcano-Gonzalez I, Paterson J, Ferguson E & Beale AM. ACS Catalysis7, 2284–2293 (2017)
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The effect of moisture on cellulose nanocrystals intended as a high gas barrier coating on flexible packaging materials. Fotie G, Rampazzo R, Ortenzi MA, Checchia S, Fessas D & Piergiovanni L. Polymers9, 415 (2017)
The emerging role of 4D synchrotron X-ray micro-tomography for climate and fossil energy studies: five experiments showing the present capabilities at beamline 8.3. 2 at the Advanced Light Source. Voltolini M, Haboub A, Dou S, Kwon T-H, MacDowell AA, Parkinson DY & Ajo-Franklin J. Journal of synchrotron radiation24, 1237–1249 (2017)
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The role of local instabilities in fluid invasion into permeable media. Singh K, Scholl H, Brinkmann M, Di Michiel M, Scheel M, Herminghaus S & Seemann R. Scientific reports7, 1–11 (2017)
The X-Ray Micro-Tomography Backed by Molecular Dynamics Simulations in the Analysis of Shock-Induced Damage in Ductile Materials. Bontaz-Carion J, Soulard L, Lescoute E, Sollier A & Berthe L. 905, 182–189 (2017)
Time resolved operando X-ray techniques in catalysis, a case study: CO oxidation by O2 over Pt surfaces and alumina supported Pt catalysts. Newton MA. Catalysts7, 58 (2017)
Understanding the residual stress distribution through the thickness of atmosphere plasma sprayed (APS) thermal barrier coatings (TBCs) by high energy synchrotron XRD; digital image correlation (DIC) and image based modelling. Li C, Zhang X, Chen Y, Carr J, Jacques S, Behnsen J, Di Michiel M, Xiao P & Cernik R. Acta materialia132, 1–12 (2017)